A Study of the Friedel-Crafts Alkylation Reaction |
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1,2,4-trichlorobenzene 2-(4-Acetoxyphenyl)ethyl Bromide 2-(4-nitrophenyl)ethyl bromide 2-phenethyl bromide 2-phenethyl chloride 4-methylbibenzyl acid evolved acid was evolved added addition aliquots alkyl halide Alkylation of toluene allowed to stand aluminum bromide aluminum chloride aromatic Beilstein test benzene benzoic acid bromide and toluene Brown bulb carbon dioxide carbonium ion catalyst CHâ‚‚ Chem chloride and toluene Combustion complex compound concentration cooled counting tube crystals distilled at reduced dried over sodium drying ethanol ethyl bromide evaporated Excess Toluene filtered flask equipped fractions were collected hydrobromic acid ibid ice water isolated isotope effect layers were separated material minutes mole mole/liter naphthalene nitrobenzene obtained organic layer Oxidation Peak Height phenethyl phenol phenylacetic acid Radioactivity Analyses reaction between 2-phenethyl REACTION BETWEEN TOLUENE reaction mixture rearrangement recrystallized reduced pressure room temperature sodium bicarbonate sodium hydroxide sodium sulfate solvent stirrer sublimed aluminum chloride sulfuric acid Three fractions tion Toluene with 2-Phenethyl trap trichlorobenzene vapor chromatograph Vigreux column